Nickel, chloro(h5-2,4-cyclopentadien-1-yl)(triphenylphosphine)-
Chloro(cyclopentadienyl)(triphenylphosphine)nickel(II)
CAS: 31904-79-7
Molecular Formula: C23H20ClNiP5*
Nickel, chloro(h5-2,4-cyclopentadien-1-yl)(triphenylphosphine)- - Names and Identifiers
Nickel, chloro(h5-2,4-cyclopentadien-1-yl)(triphenylphosphine)- - Physico-chemical Properties
| Molecular Formula | C23H20ClNiP5* |
| Molar Mass | 421.53 |
| Melting Point | 175°C (dec.)(lit.) |
| Appearance | solid |
| Storage Condition | under inert gas (nitrogen or Argon) at 2-8°C |
Nickel, chloro(h5-2,4-cyclopentadien-1-yl)(triphenylphosphine)- - Risk and Safety
| Hazard Symbols | Xn - Harmful |
| Risk Codes | 20/21/22 - Harmful by inhalation, in contact with skin and if swallowed. |
| Safety Description | 36 - Wear suitable protective clothing. |
| WGK Germany | 3 |
| HS Code | 29319090 |
Nickel, chloro(h5-2,4-cyclopentadien-1-yl)(triphenylphosphine)- - Introduction
Cyclopentadienyl triphenylphosphine nickel (II) chloride is an organometallic compound with the chemical formula (C5H5)NiCl(PPh3). The following is a description of its nature, use, preparation and safety information:
Nature:
-Appearance: Cyclopentadienyl triphenylphosphine nickel (II) chloride is a dark green crystal or powder with a special metal organic structure.
-Melting point: Its melting point is about 170-172°C.
-Solubility: Soluble in organic solvents such as ethanol, chloroform and dimethyl sulfoxide.
Use:
-Development of new catalysts: Cyclopentadienyl triphenylphosphine nickel (II) chloride is widely used in organic synthesis reactions and can be used as a catalyst to catalyze the addition reactions, reduction reactions, and halogenation reactions of carbonyl compounds.
-Metal organic chemistry research: as a model compound to study the chemical characteristics and reaction mechanism of metal organic.
Preparation Method:
Cyclopentadienyl triphenylphosphine nickel (II) chloride can be prepared by the following steps:
1. Cyclopentadienyl sodium is reacted with triphenylphosphine to obtain a cyclopentadienyl triphenylphosphine compound.
2. The above compound is reacted with nickel (II) chloride to obtain cyclopentadienyl triphenylphosphine nickel (II) chloride.
Safety Information:
-This compound is an organometallic compound and has a certain toxicity. It is necessary to comply with the corresponding safety operation regulations in the laboratory.
-Avoid inhalation or contact with skin and eyes.
-Wear suitable protective gloves and eye protection when handling this compound.
-Should be used in a well-ventilated laboratory environment.
-Store it in a sealed container, away from fire and oxidizing agents.
Nature:
-Appearance: Cyclopentadienyl triphenylphosphine nickel (II) chloride is a dark green crystal or powder with a special metal organic structure.
-Melting point: Its melting point is about 170-172°C.
-Solubility: Soluble in organic solvents such as ethanol, chloroform and dimethyl sulfoxide.
Use:
-Development of new catalysts: Cyclopentadienyl triphenylphosphine nickel (II) chloride is widely used in organic synthesis reactions and can be used as a catalyst to catalyze the addition reactions, reduction reactions, and halogenation reactions of carbonyl compounds.
-Metal organic chemistry research: as a model compound to study the chemical characteristics and reaction mechanism of metal organic.
Preparation Method:
Cyclopentadienyl triphenylphosphine nickel (II) chloride can be prepared by the following steps:
1. Cyclopentadienyl sodium is reacted with triphenylphosphine to obtain a cyclopentadienyl triphenylphosphine compound.
2. The above compound is reacted with nickel (II) chloride to obtain cyclopentadienyl triphenylphosphine nickel (II) chloride.
Safety Information:
-This compound is an organometallic compound and has a certain toxicity. It is necessary to comply with the corresponding safety operation regulations in the laboratory.
-Avoid inhalation or contact with skin and eyes.
-Wear suitable protective gloves and eye protection when handling this compound.
-Should be used in a well-ventilated laboratory environment.
-Store it in a sealed container, away from fire and oxidizing agents.
Last Update：2024-04-10 22:29:15
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Nickel, chloro(h5-2,4-cyclopentadien-1-yl)(triphenylphosphine)-
活性青莲2R
1-(叔丁氧基羰基)-4-环丙基-4-哌啶羧酸
2-(Methylamino)biphenyl
活性青莲2R
1-(叔丁氧基羰基)-4-环丙基-4-哌啶羧酸
2-(Methylamino)biphenyl